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HRID1186651

反应详情

EQUATION

反应方程式

HRID 1186651 的结构方程式

REACTANTS

反应物

2
反应SMILES：Cc1ccccc1NS(=O)(=O)c1ccc(N)cc1
HCID593569

4-Amino-N-(2-methylphenyl)benzenesulfonamide

C13H14N2O2S

反应SMILES：COc1ccc(NS(=O)(=O)c2ccc([N+](=O)[O-])cc2OC)cc1
HCID47062676

未命名化合物

PRODUCTS

产物

1
反应SMILES：COc1ccc(NS(=O)(=O)c2ccc(N)cc2OC)cc1
HCID43257464

未命名化合物

收率 77%

PROCEDURE

实验过程

(RK1-1-45) I This compound was prepared according to the procedure described for compound 12a except using 11k to obtain the required product as a yellow solid (141 mg, 77%). Mp=51-54° C.; 1H NMR (400 MHz, CDCl3) δ 7.44 (d, J=8.4 Hz, 1H), 6.97 (d, J=8.8 Hz, 2H), 6.72 (d, J=8.8 Hz, 2H), 6.61 (br s, 1H), 6.19 (d, J=2.0 Hz, 1H), 6.14 (dd, J=8.6, 2.2 Hz, 1H), 4.06 (br s, 2H), 3.98 (s, 3H), 3.72 (s, 3H).

WORKUP

后处理

  1. custom(RK1-1-45) I This compound was prepared