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HRID1186664

反应详情

EQUATION

反应方程式

HRID 1186664 的结构方程式

REACTANTS

反应物

2
结构：NS(=O)(=O)c1ccc2ccccc2c1
HCID232997

Naphthalene-2-sulfonamide

C10H9NO2S

结构：O=C1C(Cl)=C/C(=N\S(=O)(=O)c2cccs2)c2ccccc21
HCID22524852

未命名化合物

PRODUCTS

生成物

1
结构：O=C1C(Cl)=CC(=NS(=O)(=O)c2ccc3ccccc3c2)c2ccccc21
HCID7559435

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Cl][Ti]([Cl])([Cl])[Cl]
催化剂HCID24193

Titanium tetrachloride

Cl4Ti

结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

5.2.35 N-(3-chloro-4-oxonaphthalen-1(4H)-ylidene)naphthalene-2-sulfonamide (12f) was prepared according to the procedure for (12a) except using naphthalene-2-sulfonamide, TiCl4.2THF and THF as solvent which afforded the title compound 594.8 mg (77.9%) as a yellow solid, m.p.: 200-202° C.