HRID1186675

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：O=C(O)CSc1cc(NS(=O)(=O)c2cccs2)c2ccccc2c1O

HCID1582605

未命名化合物

$结构：O=C1C(Cl)=C/C(=N\S(=O)(=O)c2ccc(Cl)s2)c2ccccc21$

HCID46909450

未命名化合物

PRODUCTS

生成物

结构：O=C(O)CSc1cc(NS(=O)(=O)c2ccc(Cl)s2)c2ccccc2c1O

HCID44609306

未命名化合物

PROCEDURE

实验过程

5.2.57 2-(4-(5-chlorothiophene-2-sulfonamido)-1-hydroxynaphthalen-2-ylthio)acetic acid (14o) was prepared according to the procedure of procedure B for 10a except using (E)-5-chloro-N-(3-chloro-4-oxonaphthalen-1(4H)-ylidene)thiophene-2-sulfonamide (12d), which afforded the title compound 32.4 mg (54%) as a white solid, m.p.: 143-145° C.