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HRID1186679

反应详情

EQUATION

反应方程式

HRID 1186679 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)CSc1cc(NS(=O)(=O)c2cccs2)c2ccccc2c1O
HCID1582605

未命名化合物

结构：CCOC(=O)CSc1cc(NS(=O)(=O)c2ccc(-c3ccccc3)cc2)c2ccccc2c1O
HCID46908188

未命名化合物

PRODUCTS

生成物

1
结构：O=C(O)CSc1cc(NS(=O)(=O)c2ccc(-c3ccccc3)cc2)c2ccccc2c1O
HCID44609307

未命名化合物

PROCEDURE

实验过程

5.2.61 2-(4-(biphenyl-4-ylsulfonamido)-1-hydroxynaphthalen-2-ylthio)acetic acid (14s) was prepared according to the procedure of procedure B for 10a except using ethyl 2-(4-(biphenyl-4-ylsulfonamido)-1-hydroxynaphthalen-2-ylthio)acetate (14r) and applying r.t. overnight to the reaction, which afforded the title compound 19.2 mg (40.7%) as a grey solid, m.p.: 170° C. (dec.).

WORKUP

后处理

  1. customapplying r.t. overnight to the reaction, which