3-(5-Methyl-(1,3,4)oxadiazol-2-yl)-phenylamine → 1-Nitro-2-[3-(5-methyl-[1,3,4]oxadiazol-2-yl)phenyl]aminonaphthalene
Reaktionsgleichung
O([C:9]1[CH:18]=[CH:17][C:16]2[C:11](=[CH:12][CH:13]=[CH:14][CH:15]=2)[C:10]=1[N+:19]([O-:21])=[O:20])S(C(F)(F)F)(=O)=O.[CH3:22][C:23]1[O:27][C:26]([C:28]2[CH:29]=[C:30]([CH:32]=[CH:33][CH:34]=2)[NH2:31])=[N:25][N:24]=1>>[N+:19]([C:10]1[C:11]2[C:16](=[CH:15][CH:14]=[CH:13][CH:12]=2)[CH:17]=[CH:18][C:9]=1[NH:31][C:30]1[CH:32]=[CH:33][CH:34]=[C:28]([C:26]2[O:27][C:23]([CH3:22])=[N:24][N:25]=2)[CH:29]=1)([O-:21])=[O:20]Komponenten
3
Versuchsvorschrift
1-Nitronaphthalen-2-yl triflate (1.54 g, 4.8 mmol) and 3-(5-methyl-[1,3,4]oxadiazol-2-yl)aniline (0.84 g, 4.8 mmol) were used in a process similar to Example 1(1) to give the titled compound (1.17 g, yield 71%).
Quellen und Nachweise
- ORD-Eintrag
- ord-879bafbbcc5044829d70839fde84f861
- Quelldatensatz
- uspto-grants-2014_03
- Patentnummer
- US08673915B2
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