HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → 4-(4-tert-Butoxycarbonylaminophenyl)-1,4-dihydrobenzo[f]quinoxaline-2,3-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | tert-Butyl (4-((1-aminonaphthalen-2-yl)amino)phenyl)carbamate | HCID 86690020 | — |
| Product | 4-(4-tert-Butoxycarbonylaminophenyl)-1,4-dihydrobenzo[f]quinoxaline-2,3-dione | HCID 86690019 | 38% |
Reaction Steps
1-Amino-2-(4-tertbutoxycarbonylaminophenyl)aminonaphthalene (700 mg, 2.0 mmol) and oxalyl chloride (330 mg, 2.6 mmol) were used in a process similar to Example 1(3) to give the titled compound (304 mg, yield 38%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08673915B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-58b4f474b99d410f986cb1dd6483c9de |
| Source note | uspto-grants-2014_03 |