HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59238245, compound → (3-bromo-2,5-dimethylphenyl)methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59238245 | HCID 59238245 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | (3-bromo-2,5-dimethylphenyl)methanol | HCID 10656303 | — |
Reaction Steps
To a solution of 3-bromo-2,5-dimethylbenzoic acid (3.5 g, 15 mmol) in anhydrous THF was added borane THF complex (1.0 M, 25 mL, 25 mmol) at 0° C., then the reaction was warmed to ambient temperature overnight. The reaction was quenched with MeOH and concentrated to afford (3-bromo-2,5-dimethylphenyl)methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08673920B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-45967cbc690843e1ac8c0cb2df08461b |
| Source note | uspto-grants-2014_03 |