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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1187064Generated: November 1, 2026

HCID 59238245, compound → (3-bromo-2,5-dimethylphenyl)methanol

https://huagongshe.com/reaction/1187064

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 59238245HCID 59238245—
SolventTetrahydrofuranHCID 8028—
Product(3-bromo-2,5-dimethylphenyl)methanolHCID 10656303—

Reaction Steps

To a solution of 3-bromo-2,5-dimethylbenzoic acid (3.5 g, 15 mmol) in anhydrous THF was added borane THF complex (1.0 M, 25 mL, 25 mmol) at 0° C., then the reaction was warmed to ambient temperature overnight. The reaction was quenched with MeOH and concentrated to afford (3-bromo-2,5-dimethylphenyl)methanol.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08673920B2
Source datasetuspto-grants-2014_03
ORD IDord-45967cbc690843e1ac8c0cb2df08461b
Source noteuspto-grants-2014_03