Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Cyclohexanethiol | HCID 15290 | — |
| Reactant | HCID 59830729 | HCID 59830729 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 59830758 | HCID 59830758 | — |
Reaction Steps
Anhydrous sodium carbonate (2.201 mL, 52.58 mmol) was added in one portion to N-(2-adamantyl)-2,6-dichloro-pyridine-3-carboxamide (5.7 g, 17.53 mmol) and cyclohexyl mercaptan (2.14 mL, 17.53 mmol) in DMF (50 mL) under nitrogen. The resulting suspension was stirred at 60° C. for 6 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08673938B2 |
|---|
| Source dataset | uspto-grants-2014_03 |
|---|
| ORD ID | ord-4e70fb5864eb48eeb0602ec42eb0c5ac |
|---|
| Source note | uspto-grants-2014_03 |
|---|
