HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Dibromopropane → Ethyl 1-pyridin-3-ylcyclobutane-1-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Dibromopropane | HCID 8001 | — |
| Reactant | Ethyl 3-pyridylacetate | HCID 96490 | — |
| Product | Ethyl 1-pyridin-3-ylcyclobutane-1-carboxylate | HCID 67246748 | — |
Reaction Steps
Prepared in a similar manner to that described above by reacting ethyl 2-pyridin-3-ylacetate with 1,3-dibromopropane to give ethyl 1-pyridin-3-ylcyclobutane-1-carboxylate which was then hydrogenated to give the desired compound as a brown oil (quantitative reaction).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08673938B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-8ad4b7b25a8948c6b16f1d5fb5c1c881 |
| Source note | uspto-grants-2014_03 |