HCID 69506517, compound → HCID 69506445, compound

Participants

Reaction Steps

A mixture of 3-[(5,6-dimethyl-8-nitrotetraazolo[1,5-a]pyridin-7-yl)amino]propyl acetate (0.43 g, 1.4 mmol) and 10% platinum on carbon (43 mg) in acetonitrile (14 iL) was hydrogenated at 50 psi (3.5×105 Pa) on a Parr apparatus for 3 hours. The mixture was filtered through CELITE filter agent, which was rinsed with chloroform. The filtrate was concentrated under reduced pressure to yield 0.36 g of 3-[(8-amino-5,6-dimethyltetraazolo[1,5-a]pyridin-7-yl)amino]propyl acetate as a white solid.

Provenance & Evidence