3-Chloropropiophenone → HCID 10214453, compound

HRID 1187882Notes

Reaction equation

HRID 1187882 reaction equation
[Cl:1][CH2:2][CH2:3][C:4]([C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1)=[O:5].[CH2:12]([Mg]Br)[CH3:13]>>[Cl:1][CH2:2][CH2:3][C:4]([C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1)([OH:5])[CH2:12][CH3:13]

Participants

3

Reactant 2

HCID 702953-ChloropropiophenoneHCID 178418443HCID 178418443, compound

Product 1

HCID 10214453HCID 10214453, compound

Procedure

1-chloro-3-phenylpentan-3-ol was prepared from 3-chloro-1-phenylpropan-1-one and ethylmagnesium bromide following a procedure analogous to that described in Preparation 1 Method 1 Step 2.

Workup

  1. customthat described in Preparation 1 Method 1 Step 2

Sources & evidence

ORD record
ord-672caeab027449e29122ee042046bbf6
Source dataset
uspto-grants-2014_03
Patent number
US08673899B2

Reaction notes

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