Chloroform ethylacetate → HCID 86674621, compound

Participants

Reaction Steps

N-Benzyl-5-((5-p-tolylthiazol-2-ylamino)methyl)thiazol-2-amine (20 mg, 0.05 mmol) was dissolved in methanolic HCl (3 N, 1 mL) and CHCl3/AcOEt was added. The precipitated solid was filtered by decantation and dried in vacuo, yielding N-benzyl-5-((5-p-tolylthiazol-2-ylamino)methyl)thiazol-2-amine dihydrochloride as a white solid (11 mg, 10%). Mp. 105-106° C.

Provenance & Evidence