Lawesson's reagent → HCID 58236986, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 7-methoxy-5-[4-(methylsulfonyl)phenoxy]-1H-indole-2-carboxamide (0.73 g) and Lawesson's reagent (0.49 g) in tetrahydrofuran (30 mL) was stirred at 55° C. for 3 h. The reaction mixture was concentrated to give a light yellow oil, which was crystallized from ethyl acetate-hexane to give the title compound (691 mg, 91%) as light yellow prisms. MS 375 (MH+).

Provenance & Evidence