HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromopyridine → HCID 11652241, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromopyridine | HCID 7973 | — |
| Reactant | HCID 86086862 | HCID 86086862 | — |
| Product | HCID 11652241 | HCID 11652241 | 17,931% |
Reaction Steps
The title compound was prepared in accordance with the general method of Example 1, from 2-bromopyridine (46 mg, 0.29 mmol) and 2-but-3-ynyl-4,7-dimethyl-benzo[d]thiazole (63 mg, 0.29 mmol). The crude residue was purified by flash chromatography (DCM/MeOH 99:1 to 98:2) to yield 15 mg (52 mmol, 18%) of 4,7-dimethyl-2-(4-(pyridin-2-yl)but-3-ynyl)benzo[d]thiazole as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08674106B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-cf6cd0aecfc04d64a4482a3ac6b3989d |
| Source note | uspto-grants-2014_03 |