Aluminium lithium hydride → HCID 56839970, compound

HRID 1189622Notes

Reaction equation

HRID 1189622 reaction equation
[NH2:1][C:2]1[C:3]([F:12])=[C:4]([CH:8]=[CH:9][C:10]=1[Cl:11])[C:5]([NH2:7])=O.[H-].[H-].[H-].[H-].[Li+].[Al+3]>>[NH2:1][C:2]1[C:3]([F:12])=[C:4]([CH:8]=[CH:9][C:10]=1[Cl:11])[CH2:5][NH2:7]

Participants

3

Reactant 2

HCID 21226445Aluminium lithium hydrideHCID 667651113-Amino-4-chloro-2-fluoro-benzamide

Product 1

HCID 56839970HCID 56839970, compound

Procedure

The crude sub-title compound is prepared from 3-amino-4-chloro-2-fluoro-benzamide and LiAlH4 in analogy to step Ad. HPLC-method B: Rt=0.37 min. MS m/z: 175 [M+H]+.

Sources & evidence

ORD record
ord-912f8caaeea3470a880eaaea8ed55e39
Source dataset
uspto-grants-2014_03
Patent number
US08674113B2

Reaction notes

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