HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-Isopropyl-piperazin-1-yl)-5-nitro-pyrimidine → HCID 61146131, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-Isopropyl-piperazin-1-yl)-5-nitro-pyrimidine | HCID 66914667 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 61146131 | HCID 61146131 | — |
Reaction Steps
The title compound was prepared in analogy to the procedure described in Step 33.1 but using 2-(4-isopropyl-piperazin-1-yl)-5-nitro-pyrimidine (Step 35.2) and stirring the reaction mixture for 1.5 h. The title compound: ESI-MS: 222.1 [M+H]+; TLC: Rf=0.13 (DCM/MeOH/NH3aq, 94:5:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08674099B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-3960a1afdadc4e6c8031bf732ff4dbcc |
| Source note | uspto-grants-2014_03 |