HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Cyclohexenylboronic acid → Acetic acid 3-acetoxy-2-(4-amino-3-cyclohex-1-enyl-phenyl)-propyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Cyclohexenylboronic acid | HCID 3862902 | — |
| Reactant | Acetic acid 3-acetoxy-2-(4-amino-3-bromo-phenyl)-propyl ester | HCID 67187511 | — |
| Product | Acetic acid 3-acetoxy-2-(4-amino-3-cyclohex-1-enyl-phenyl)-propyl ester | HCID 59771138 | — |
Reaction Steps
The title compound was prepared according to the Suzuki coupling procedure of Example 1, step (e) using acetic acid 3-acetoxy-2-(4-amino-3-bromo-phenyl)-propyl ester (as prepared above) and cyclohex-1-enyl boronic acid: Mass spectrum, (ESI, m/z): Calcd. for C19H25NO4, 332.1 (M+H). found 332.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08674100B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-7601d151c347442e9e563774b6960789 |
| Source note | uspto-grants-2014_03 |