HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 90773835, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | 2-Methoxyethylamine | HCID 8018 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 59457539 | HCID 59457539 | — |
| Product | HCID 90773835 | HCID 90773835 | — |
Reaction Steps
The title compound is prepared from 5-cyano-1H-imidazole-2-carboxylic acid [2-(4,4-dimethyl-cyclohex-1-enyl)-6-(1-hydroxy-1-methyl-ethyl)-pyridin-3-yl]-amide (as prepared in Example 59, step (e)), methoxyethylamine and thionyl chloride in DCM solvent according to the procedure in Example 14, step (e).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08674100B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-bbe2c555c0d144bbb015c9db51b8cbb4 |
| Source note | uspto-grants-2014_03 |