HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57702611, compound → Naphthalene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57702611 | HCID 57702611 | — |
| Reactant | HCID 59760676 | HCID 59760676 | — |
| Product | Naphthalene | HCID 931 | — |
Reaction Steps
Preparation analogous to Example 3b. Instead of 19.5 g (40 mmol) of 9,10-bis(2-bromophenyl)anthracene, 25.5 g (40 mmol) of 1,4-bis(10-bromoanthracen-9-yl)naphthalene are used. Sublimation at p=1×10−5 mbar, T=300° C. Yield: 12.1 g (16.5 mmol), 41.3% of theory; purity: 99.8% according to 1H-NMR.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08674141B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-8228f54cd55b4f4eb2d361cba2e2e148 |
| Source note | uspto-grants-2014_03 |