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HRID1190305

反应详情

EQUATION

反应方程式

HRID 1190305 的结构方程式

REACTANTS

反应物

3
结构：CC(NN)C(F)(F)F
HCID20541215

未命名化合物

结构：FC(F)(F)Cn1ncnc1-c1nc2c(s1)CCOc1cc(Br)ccc1-2
HCID58203849

8-Bromo-2-[2-(2,2,2-trifluoro-ethyl)-2H-[1,2,4]triazol-3-yl]-4,5-dihydro-6-oxa-3-thia-1-aza-benzo[e]azulene

C15H10BrF3N4OS

结构：NC(=O)c1nc2c(s1)CCOc1cc(Br)ccc1-2
HCID67050530

未命名化合物

PRODUCTS

生成物

1
结构：CC(n1ncnc1-c1nc2c(s1)CCOc1cc(Br)ccc1-2)C(F)(F)F
HCID58203738

未命名化合物

PROCEDURE

实验过程

Following the procedure for 8-Bromo-2-[2-(2,2,2-trifluoro-ethyl)-2H-[1,2,4]triazol-3-yl]-4,5-dihydro-6-oxa-3-thia-1-aza-benzo[e]azulene, 8-Bromo-4,5-dihydro-6-oxa-3-thia-1-aza-benzo[e]azulene-2-carboxylic acid amide 25 was reacted with (2,2,2-Trifluoro-1-methyl-ethyl)-hydrazine to give 8-Bromo-2-[2-(2,2,2-trifluoro-1-methyl-ethyl)-2H-[1,2,4]triazol-3-yl]-4,5-dihydro-6-oxa-3-thia-1-aza-benzo[e]azulene. MS (ESI+) 445.0/447.0.