HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-pyridin-4-yl-1,4-diazepane → HCID 58203764, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-pyridin-4-yl-1,4-diazepane | HCID 2760508 | — |
| Reactant | 8-(1H-Pyrazol-4-yl)-4,5-dihydro-6-oxa-3-thia-1-aza-benzo[e]azulene-2-carboxylic acid | HCID 58203883 | — |
| Product | HCID 58203764 | HCID 58203764 | — |
Reaction Steps
Following the procedure for 103, 8-(1H-Pyrazol-4-yl)-4,5-dihydro-6-oxa-3-thia-1-aza-benzo[e]azulene-2-carboxylic acid (50.0 mg, 0.2 mmol) was reacted with 1-(pyridin-4-yl)-1,4-diazepane (1.2 equiv) to give 208 (M+1 473.0)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08673952B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-e640129b34c34a03b15d8a1a1e6679f4 |
| Source note | uspto-grants-2014_03 |