HCID 86634383, compound → HCID 86634384, compound

Participants

Reaction Steps

The compound 19 (225 mg), acetic acid (4 mL) and 10% palladium carbon (20 mg) were stirred under hydrogen atmosphere at room temperature for 6 hours. The reaction solution was filtered and then the filtrate was concentrated. The residue was added aqueous 2N sodium hydroxide solution and extracted with dichloromethane. The extract was dried over anhydrous magnesium sulfate, concentrated and obtained the title compound (155 mg) having the following physical properties.

Provenance & Evidence