HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetyl chloride → 8-Isopropyl-4H-benzo[1,4]oxazin-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetyl chloride | HCID 6577 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Amino-6-isopropylphenol | HCID 14684982 | — |
| Product | 8-Isopropyl-4H-benzo[1,4]oxazin-3-one | HCID 68912176 | — |
Reaction Steps
Crude 2-Amino-6-isopropylphenol (95MF80(2240) (0.16 g, 1.1 mmol), 2-chloroacetyl chloride (0.14 g, 1.2 mmol) and K2CO3 (0.32 g, 2.3 mmol) were mixed according to GP1 to give the title compound as a crude (95MF83) (0.115 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680115B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-80ff3b87b75840fb85d7a5d9571f6d83 |
| Source note | uspto-grants-2014_03 |