HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetyl chloride → 6,8-Dichloro-7-methyl-4H-benzo[1,4]oxazin-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetyl chloride | HCID 6577 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Amino-4,6-dichloro-5-methylphenol | HCID 170224 | — |
| Product | 6,8-Dichloro-7-methyl-4H-benzo[1,4]oxazin-3-one | HCID 68912189 | — |
Reaction Steps
6-Amino-2.4 dichloro-3-methylphenol (1.9 g, 10 mmol), 2-chloroacetyl chloride (1.2 g, 11 mmol) and K2CO3 (3.0 g, 22 mmol) were mixed according to GP1 to give the title compound as a crude (80MF2225) (2.33 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680115B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-2a7100becf1641268b68fc67bbb12763 |
| Source note | uspto-grants-2014_03 |