Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1191476Generated: November 1, 2026

Sodium Iodide → HCID 68908797, compound

https://huagongshe.com/reaction/1191476

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium IodideHCID 5238—
ReactantDimethylformamideHCID 6228—
ReactantPotassium CarbonateHCID 11430—
Reactant3-Pentyl-8-azabicyclo[3.2.1]octaneHCID 21989852—
ProductHCID 68908797HCID 68908797—

Reaction Steps

Crude (R,S)-1-(3-chloro-2-methylpropyl)-3,4-dihydro-1H-quinolin-2-one (107LH63) (0.094 g), 3-pentyl-8-azabicyclo[3.2.1]octane (0.027 g, 0.15 mmol), NaI (0.100 g, 0.67 mmol), and K2CO3 (0.075 g, 0.54 mmol) in DMF (1 mL) were reacted and purified according to GP20 to give the title compound (107LH74-c5) (0.023 g). HPLC-MS (ammonium acetate) [M+H]+=383.34.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08680115B2
Source datasetuspto-grants-2014_03
ORD IDord-f3e14ea4930b4096a8e0738409e9daed
Source noteuspto-grants-2014_03