HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron Trichloride → Bnc-105
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron Trichloride | HCID 25135 | — |
| Reactant | 2-Methyl-3-(3,4,5-trimethoxybenzoyl)-6-methoxy-7-isopropoxy-benzo[b]furan | HCID 60149020 | — |
| Product | Bnc-105 | HCID 24786555 | 83% |
Reaction Steps
Note: A similar reaction when scaled-up with 2-methyl-3-(3,4,5-trimethoxybenzoyl)-6-methoxy-7-isopropoxy-benzo[b]furan (1.25 gm) and boron trichloride solution (1M solution in DCM, 3.1 mL) gave the title compound (930 mg, 83%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680135B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-5334993856094fc78377e9a27c9aa3cc |
| Source note | uspto-grants-2014_03 |