HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichlorobenzenethiol → 1-[5-(2,4-Dichlorophenylsulfanyl)-4-nitro-2-thienyl]ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichlorobenzenethiol | HCID 70730 | — |
| Reactant | 1-(5-Chloro-4-nitrothiophen-2-yl)ethan-1-one | HCID 521105 | — |
| Product | 1-[5-(2,4-Dichlorophenylsulfanyl)-4-nitro-2-thienyl]ethanone | HCID 46931952 | — |
Reaction Steps
Prepared according to the procedure described as in Step B for example 1 from 1-(5-Chloro-4-nitro-2-thienyl)ethanone (0.164 g, 0.8 mmol) and 2,4-dichlorobenzenethiol (0.143 g, 0.8 mmol). The title compound was obtained as an orange solid (132 mg, 47.3% yield). 1H NMR (300 MHz, CDCl3) δ: 8.09 (1H, s), 7.68 (2H, m), 7.42 (1H, d), 2.50 (3H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680139B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-1ef9640364a44f56aaca78483f670405 |
| Source note | uspto-grants-2014_03 |