HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chlorothiophenol → 1-[5-(3-Chlorophenylsulfanyl)-4-nitro-2-thienyl]ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chlorothiophenol | HCID 16257 | — |
| Reactant | 1-(5-Chloro-4-nitrothiophen-2-yl)ethan-1-one | HCID 521105 | — |
| Product | 1-[5-(3-Chlorophenylsulfanyl)-4-nitro-2-thienyl]ethanone | HCID 46931956 | — |
Reaction Steps
Prepared according to the procedure described as in Step B for example 1 from 1-(5-Chloro-4-nitro-2-thienyl)ethanone (0.502 g, 2.45 mmol) and 3-chlorobenzenethiol (0.353 g, 2.45 mmol). The title compound was obtained as a yellow solid (0.476 g, 62% yield). 1H NMR (300 MHz, CDCl3) δ: 8.08 (1H, s), 7.68 (1H, m), 7.45-7.60 (3H, m), 2.49 (3H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680139B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-01c1ca3c6b5040ae8b21aa0b21fa499b |
| Source note | uspto-grants-2014_03 |