1-(5-Chloro-4-nitrothiophen-2-yl)ethan-1-one → 1-(5-((3,5-Dichlorophenyl)thio)-4-nitrothiophen-2-yl)ethanone

Participants

Reaction Steps

Prepared according to the procedure described as in Step B for example 1 from 1-(5-Chloro-4-nitro-2-thienyl)ethanone (0.502 g, 2.45 mmol) and 3,5-dichlorobenzenethiol (0.438 g, 2.45 mmol). The title compound was obtained as a yellow solid (0.403 g, 47.5% yield). 1H NMR (300 MHz, CDCl3) δ: 8.08 (1H, s), 7.57 (3H, m), 2.51 (3H, s).

Provenance & Evidence