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HRID1192067

反应详情

EQUATION

反应方程式

HRID 1192067 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)c1cc([N+](=O)[O-])c(Cl)s1
HCID521105

1-(5-Chloro-4-nitrothiophen-2-yl)ethan-1-one

C6H4ClNO3S

结构：Sc1cnc2ccccc2n1
HCID178418602

未命名化合物

PRODUCTS

生成物

1
结构：CC(=O)c1cc([N+](=O)[O-])c(Sc2cnc3ccccc3n2)s1
HCID46932326

未命名化合物

PROCEDURE

实验过程

Prepared according to the procedure described for example 18 from 1-(5-Chloro-4-nitro-2-thienyl)ethanone (250 mg, 1.215 mmol) and quinoxaline-2-thiol (197 mg, 1.215 mmol). The title compound was obtained as a solid (200 mg, 50% yield). 1H NMR (400 MHz, d6-DMSO) δ: 9.26 (1H, s), 8.63 (1H, s), 8.01 (1H, m), 7.98 (1H, m), 2.61 (3H, s). MS m/z: 331.88 [M+H]+.

WORKUP

后处理

  1. customPrepared