Furfurylamine → HCID 46932517, compound

Participants

Reaction Steps

Prepared according to the procedure described for example 50 from 5-[(3,5-dichloro-4-pyridyl)sulfanyl]-4-nitro-thiophene-2-carboxylic acid (100 mg, 0.27 mmol) and Furfuryl amine (31 mg, 0.32 mmol). The title compound was obtained as a solid (45 mg, 39% yield). 1H NMR (400 MHz, d6-DMSO) δ: 9.34 (1H, m), 8.99 (2H, m), 8.48 (1H, s), 7.58 (1H, m), 6.39 (1H, m), 6.29 (1H, m), 4.39 (2H, m). MS m/z: 428.04, 429.99 [M+H]+.

Provenance & Evidence