Isoamylamine → HCID 60207346, compound

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Reaction Steps

Prepared according to the procedure described for example 50 from 5-[(3,5-dichloro-4-pyridyl)sulfanyl]-4-nitro-thiophene-2-carbonyl chloride (150 mg, 0.41 mmol) and 3-methylbutylamine (43 mg, 0.49 mmol). The title compound was obtained as a solid (40 mg, 23% yield). 1H NMR (400 MHz, d6-DMSO) δ: 8.98 (2H, s), 8.76 (1H, m), 8.42 (1H, s), 3.21 (2H, t), 1.58 (1H, m), 1.37 (2H, m), 0.93 (6H, m). MS m/z: 418.06, 420.08 [M+H]+.

Provenance & Evidence