4-Bromobenzylamine → HCID 60207354, compound

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Reaction Steps

Prepared according to the procedure described for example 50 from 5-[(3,5-dichloro-4-pyridyl)sulfanyl]-4-nitro-thiophene-2-carbonyl chloride (150 mg, 0.41 mmol) and 4-bromo-benzylamine (91 mg, 0.49 mmol). The title compound was obtained as a yellow solid (19 mg, 35% yield). 1H NMR (400 MHz, d6-DMSO) δ: 9.41 (1H, m), 8.99 (2H, s), 8.46 (1H, s), 7.53 (2H, dd), 7.24 (2H, dd), 4.43 (2H, m). MS m/z: 515.93, 517.96, 519.92 [M+H]+.

Provenance & Evidence