2-Methyl-4-methoxyaniline → HCID 60207368, compound

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Reaction Steps

Prepared according to the procedure described for example 50 from 5-[(3,5-dichloro-4-pyridyl)sulfanyl]-4-nitro-thiophene-2-carbonyl chloride (120 mg, 0.33 mmol) and 4-methoxy-2-methylaniline (53 mg, 0.39 mmol). The title compound was obtained as a solid (75 mg, 49% yield). 1H NMR (400 MHz, d6-DMSO) δ: 10.12(1H, s), 9.00 (2H, s), 8.63 (1H, m), 7.12 (1H, dd), 6.83 (1H, m), 6.76 (1H, m), 3.73 (3H, s), 2.14 (3H, s). MS m/z: 468.15, 470.12 [M+H]+.

Provenance & Evidence