HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenamine, 4-(4-morpholinyl)- → HCID 60207386, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenamine, 4-(4-morpholinyl)- | HCID 75655 | — |
| Reactant | 5-((3,5-Dichloropyridin-4-yl)thio)-4-nitrothiophene-2-carbonyl chloride | HCID 60207337 | — |
| Product | HCID 60207386 | HCID 60207386 | — |
Reaction Steps
Prepared according to the procedure described for example 50 from 5-[(3,5-dichloro-4-pyridyl)sulfanyl]-4-nitro-thiophene-2-carbonyl chloride (120 mg, 0.33 mmol) and 4-morpholinoaniline (69 mg, 0.39 mmol). The title compound was obtained as a solid (70 mg, 44% yield). 1H NMR (400 MHz, d6-DMSO) δ: 10.41 (1H, m), 9.00 (2H, s), 8.67 (1H, s), 7.51 (2H, m), 6.94 (2H, m), 3.72 (4H, m), 3.06 (4H, m). MS m/z: 509.15, 511.13 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680139B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-f34685cbcfb94469b7b76694fabc04d2 |
| Source note | uspto-grants-2014_03 |