p-Aminoacetophenone → HCID 60207407, compound

Participants

Reaction Steps

Prepared according to the procedure described for example 50 from 5-((3,5-dichloropyridin-4-yl)thio)-4-nitrothiophene-2-carbonyl chloride (0.25 mg, 0.59 mmol) and 1-(4-aminophenyl)ethanone (88 mg, 0.65 mmol). The title compound was obtained as a solid (27.0 mg, 10% yield). 1H NMR (400 MHz, d6-DMSO) δ: 10.78 (1H, s), 9.01 (2H, s), 8.75 (1H, m), 8.01 (2H, m), 7.82 (2H, m), 2.51 (3H, s). MS m/z: 466.03, 468.03 [M+H]+.

Provenance & Evidence