Benzylamine → HCID 60207481, compound

HRID 1192260Notes

Reaction equation

HRID 1192260 reaction equation
[S:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[S:10][C:11]1[S:15][C:14]([C:16]([OH:18])=O)=[CH:13][C:12]=1[N+:19]([O-:21])=[O:20].[CH2:22]([NH2:29])[C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1>>[S:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[S:10][C:11]1[S:15][C:14]([C:16]([NH:29][CH2:22][C:23]2[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=2)=[O:18])=[CH:13][C:12]=1[N+:19]([O-:21])=[O:20]

Participants

3

Reactant 2

HCID 7504BenzylamineHCID 60207480HCID 60207480, compound

Product 1

HCID 60207481HCID 60207481, compound

Procedure

Prepared according to the procedure described for example 44 from 5-(1,3-benzothiazol-2-ylsulfanyl)-4-nitro-thiophene-2-carboxylic acid (34 mg, 0.1 mmol) and benzylamine (13.0 mg, 0.12 mmol). The title compound was obtained as a solid (10 mg, 23% yield). MS m/z: 428.08 [M+H]+.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-5a0af677bc8d4f00ba0e69bdf6459647
Source dataset
uspto-grants-2014_03
Patent number
US08680139B2

Reaction notes

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