Benzenethiol, 2,6-dichloro- → HCID 60207504, compound

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Reaction Steps

Prepared according to the procedure described for step A of example 18 from methyl 5-chloro-4-nitrothiophene-2-carboxylate (5 g, 22.7 mmol) and 2,6-dichlorothiophenol (4.4 g, 24.8 mmol), The titled product was obtained as an off-white solid (5.5 g, 67% yield). 1H NMR (400 MHz, d6-DMSO) δ: 8.17 (1H, s), 7.83 (2H, m), 7.62 (1H, m), 3.77 (3H, s). MS m/z: 363.92, 365.93 [M+H]+.

Provenance & Evidence