1-(5-Chloro-4-nitrothiophen-2-yl)ethan-1-one → HCID 60207511, compound

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Reaction Steps

Prepared by a similar procedure to that described for example 1 from the 1-(5-chloro-4-nitro-2-thienyl)ethanone (205 mg, 1.0 mmol) and 2,3,5,6-tetrafluoro-4-chloro-benzenethiol (216 mg, 0.98 mmol) to afford the title product as a solid (220 mg, 57% yield). 1H NMR (400 MHz, d6-DMSO) δ: 8.55 (1H, s), 3.37 (3H, s). MS m/z: 384.12, 386.12 [M+H]+.

Provenance & Evidence