HCID 86656157, compound → HCID 67301543, compound

Participants

Reaction Steps

A mixture of 2-(1-azidoethyl)-1-(3-fluorophenyl)naphthalene (0.035 g, 0.12 mmol) in 1 mL of methanol was hydrogenated in the presence of 5% Pd/C, under balloon pressure of hydrogen, for 1 hour. After filtering off the catalyst, the filtrate was concentrated under reduced pressure and the resulting residue was used directly in next step. LCMS calculated for C18H14F(M−NH2)+: m/z=249.1; found: 249.3.

Provenance & Evidence