HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Formylphenylboronic Acid → HCID 57824450, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Formylphenylboronic Acid | HCID 591073 | — |
| Reactant | HCID 43654761 | HCID 43654761 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 57824450 | HCID 57824450 | — |
Reaction Steps
The compound was prepared by palladium-catalyzed arylation of the product of step 1 with 4-formylphenyl boronic acid: 1H NMR (400 MHz, CDCl3) δ 10.13 (s, 1H), 8.91 (d, J=4.8 Hz, 1H), 8.74 (d, J=8.5 Hz, 2H), 8.28 (d, J=8.4 Hz, 2H), 8.03 (d, J=8.4 Hz, 2H), 7.65 (d, J=5.3 Hz, 1H), 7.39 (d, J=8.6 Hz, 2H); EIMS m/z 344 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680269B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-33a3140305ec47378695c8c0167244fb |
| Source note | uspto-grants-2014_03 |