HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 3-(2-Methoxy-2-oxoethyl)-1,1-dimethyl-3-(5-phenethylfuran-2-carboxamido)-piperidinium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Methyl 2-(1-methyl-3-(5-phenethylfuran-2-carboxamido)piperidin-3-yl)acetate | HCID 66864596 | — |
| Product | 3-(2-Methoxy-2-oxoethyl)-1,1-dimethyl-3-(5-phenethylfuran-2-carboxamido)-piperidinium iodide | HCID 86649844 | — |
Reaction Steps
According to the method described in example 2a, methyl 2-(1-methyl-3-(5-phenethyl-furan-2-carboxamido)piperidin-3-yl)acetate was reacted with methyl iodide to give the title compound as a white solid (quantitative). MS ESI 399.2 [M]+, calcd for [C23H31N2O4]+ 399.21.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680282B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-c58ce349d3254df795a4beab42c512cb |
| Source note | uspto-grants-2014_03 |