HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Nitropropane → HCID 58434562, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Nitropropane | HCID 7903 | — |
| Reactant | Pentanal, 5,5-dimethoxy- | HCID 170903 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 58434562 | HCID 58434562 | 55.1% |
Reaction Steps
Prepared according to the general procedure A from 1-nitropropane 112c (80 mmol) and 5,5-dimethoxypentanal 131 (16 mmol) to provide the title compound as yellow oil (1.51 g, 55% yield) after silica gel chromatography (EtOAc/Hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680335B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-3e68881140b244c592c28c2896235107 |
| Source note | uspto-grants-2014_03 |