HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pentanal, 5,5-dimethoxy- → HCID 58434611, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pentanal, 5,5-dimethoxy- | HCID 170903 | — |
| Reactant | HCID 11183809 | HCID 11183809 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 58434611 | HCID 58434611 | 43% |
Reaction Steps
Prepared according to the general procedure B from 1-bromo-4-(2-nitroethyl)benzene 112h (24 mmol) and 5,5-dimethoxypentanal 131 (16 mmol) to provide the title compound as yellow oil (2.15 g, 43% yield) after silica gel chromatography (EtOAc/Hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680335B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-3c11bd458cd142a999778d326ba23204 |
| Source note | uspto-grants-2014_03 |