o-Phenylbenzoic acid → HCID 67116634, compound
Reaction equation
[C:1]1(C2C=CC=CC=2)[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[C:7]([N:9]1[CH2:15][CH:14]2[CH:11]([CH2:12][NH:13]2)[CH2:10]1)=[O:8].C1(C2C=CC=CC=2)C([C:28](O)=[O:29])=CC=CC=1>>[CH:11]12[CH2:12][NH:13][CH:14]1[CH2:15][N:9]([C:7]([C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][C:1]=1[O:29][CH3:28])=[O:8])[CH2:10]2Participants
3
Procedure
The title compound was prepared in a manner analogous to Intermediate 19, substituting 2-methoxybenzoic acid for biphenyl-2-carboxylic acid. MS (ESI) mass calcd. for C13H16N2O2, 232.28; m/z found, 233.2 [M+H]+.
Sources & evidence
- ORD record
- ord-964011b8cda442639ac765578be36ffd
- Source dataset
- uspto-grants-2014_03
- Patent number
- US08680275B2
Reaction notes
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