o-Phenylbenzoic acid → HCID 67116914, compound

HRID 1193077Notes

Reaction equation

HRID 1193077 reaction equation
[C:1]1([C:16]2[CH:21]=[CH:20][CH:19]=CC=2)[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[C:7]([N:9]1[CH2:15][CH:14]2[CH:11]([CH2:12][NH:13]2)[CH2:10]1)=[O:8].C1(C2C=CC=CC=2)[C:23]([C:28](O)=[O:29])=CC=CC=1>>[CH:11]12[CH2:12][NH:13][CH:14]1[CH2:15][N:9]([C:7]([C:2]1[C:1]3[C:6](=[CH:19][CH:20]=[CH:21][CH:16]=3)[CH:5]=[CH:4][C:3]=1[O:29][CH2:28][CH3:23])=[O:8])[CH2:10]2

Participants

3

Reactant 2

HCID 70357o-Phenylbenzoic acidHCID 67116907HCID 67116907, compound

Product 1

HCID 67116914HCID 67116914, compound

Procedure

The title compound was prepared in a manner analogous to Intermediate 19, substituting 2-ethoxy-naphthalene-1-carboxylic acid for biphenyl-2-carboxylic acid. MS (ESI) mass calcd. for C18H20N2O2, 296.37; m/z found, 297.2 [M+H]+.

Sources & evidence

ORD record
ord-8e2687bc5bd642efb2da08081c6c26f0
Source dataset
uspto-grants-2014_03
Patent number
US08680275B2

Reaction notes

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