o-Phenylbenzoic acid → HCID 69932060, compound

HRID 1193078Notes

Reaction equation

HRID 1193078 reaction equation
C1(C2C=CC=CC=2)C=CC=CC=1C([N:9]1[CH2:15][CH:14]2[CH:11]([CH2:12][NH:13]2)[CH2:10]1)=O.[CH3:22][C:23]1[CH:24]=[CH:25][C:26]([N:32]2[N:36]=[CH:35][CH:34]=[N:33]2)=[C:27]([CH:31]=1)[C:28]([OH:30])=O.C1(C2C=CC=CC=2)C(C(O)=O)=CC=CC=1>>[CH:11]12[CH2:12][NH:13][CH:14]1[CH2:15][N:9]([C:28]([C:27]1[CH:31]=[C:23]([CH3:22])[CH:24]=[CH:25][C:26]=1[N:32]1[N:36]=[CH:35][CH:34]=[N:33]1)=[O:30])[CH2:10]2

Participants

4

Reactant 3

HCID 70357o-Phenylbenzoic acidHCID 532601655-methyl-2-(2H-1,2,3-triazol-2-yl)benzoic acidHCID 67116907HCID 67116907, compound

Product 1

HCID 69932060HCID 69932060, compound

Procedure

The title compound was prepared in a manner analogous to Intermediate 19, substituting 5-methyl-2-[1,2,3]triazol-2-yl-benzoic acid (Intermediate 59) for biphenyl-2-carboxylic acid. MS (ESI) mass calcd. for C15H17N5O, 283.33; m/z found, 284.2 [M+H]+.

Sources & evidence

ORD record
ord-00eb112f31e44b8f8648f3b21b75daa0
Source dataset
uspto-grants-2014_03
Patent number
US08680275B2

Reaction notes

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