HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Fluoro-2-iodobenzoic acid → 5-Iodo-2-[1,2,3]triazol-2-yl-benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Fluoro-2-iodobenzoic acid | HCID 13158583 | — |
| Reactant | 5-fluoro-2-(2H-1,2,3-triazol-2-yl)benzoic acid | HCID 67086948 | — |
| Product | 5-Iodo-2-[1,2,3]triazol-2-yl-benzoic acid | HCID 67086732 | — |
Reaction Steps
The title compound was prepared in a manner analogous to Intermediate 13, substituting 2-bromo-5-iodobenzoic acid for 5-fluoro-2-iodo-benzoic acid in Step A. 1H NMR (400 MHz, CD3OD): 8.09 (d, J=2.0, 1H), 8.03-7.97 (m, 1H), 7.95-7.86 (m, 3H), 7.53 (d, J=8.4, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08680275B2 |
| Source dataset | uspto-grants-2014_03 |
| ORD ID | ord-252eaccabb4a43a9ba8a4c2cdbade3eb |
| Source note | uspto-grants-2014_03 |