Methyl iodide → Methyl (3-phenylpropyl)carbamodithioate

HRID 1193593Notes

Reaction equation

[C:1]1([CH2:7][CH2:8][CH2:9][NH2:10])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:11](=[S:13])=[S:12].I[CH3:15]>>[C:1]1([CH2:7][CH2:8][CH2:9][NH:10][C:11](=[S:13])[S:12][CH3:15])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

Reactant 3

HCID 6328Methyl iodide

HCID 6348Carbon Disulfide

HCID 162593-Phenylpropylamine

Product 1

HCID 14581310Methyl (3-phenylpropyl)carbamodithioateYield 94.1%

Procedure

3-Phenyl-1-propylamine (0.074 mol) was reacted with carbon disulfide (0.074 mol) and iodomethane (0.074 mol) substantially as described in Example 1B above to obtain 15.7 g (94%) of a yellow oil.

Sources & evidence

ORD record: ord-f4ae3e46dc0140e9953f78b67d6b4b43
Source dataset: uspto-grants-1989_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04810811

Reaction notes

Loading…