HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Toluenesulfonyl chloride → 3-(3,5-Dichlorophenyl)propylazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | 3,5-Dichlorobenzenepropanol | HCID 14581315 | — |
| Product | 3-(3,5-Dichlorophenyl)propylazide | HCID 14581316 | 98% |
Reaction Steps
3-(3,5-Dichlorophenyl)propanol (0.052 mol), tosyl chloride (0.104 mol) and sodium azide (0.104 mol) were reacted substantially as described in Example 7E to obtain 11.7 g (98%) of an oily product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04810811 |
| Source dataset | uspto-grants-1989_03 |
| ORD ID | ord-69b5315574bf454ab24eb758b562af51 |
| Source note | uspto-grants-1989_03 |